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Information card for entry 7111438
Preview
Coordinates | 7111438.cif |
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Original paper (by DOI) | HTML |
Common name | 1,3-Di-tert.butyl-2-chloro-1,3,2-diazastibolene |
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Chemical name | 1,3-Di-tert.butyl-2-chloro-1,3,2-diazastibolene |
Formula | C10 H20 Cl N2 Sb |
Calculated formula | C10 H20 Cl N2 Sb |
Title of publication | Synthesis and unprecedented oxidation of a cationic Sb-analogue of an Arduengo's carbene |
Authors of publication | Gudat, Dietrich; Gans-Eichler, Timo; Nieger, Martin |
Journal of publication | Chemical Communications |
Year of publication | 2004 |
Journal issue | 21 |
Pages of publication | 2434 - 2435 |
a | 11.5242 ± 0.0005 Å |
b | 10.9946 ± 0.0004 Å |
c | 21.098 ± 0.0009 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2673.2 ± 0.19 Å3 |
Cell temperature | 123 ± 2 K |
Ambient diffraction temperature | 123 ± 2 K |
Number of distinct elements | 5 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.0627 |
Residual factor for significantly intense reflections | 0.0375 |
Weighted residual factors for significantly intense reflections | 0.0826 |
Weighted residual factors for all reflections included in the refinement | 0.0911 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.933 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7111438.html
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