Information card for entry 7111508

Structure parameters

• Formula: C48 H88 Ce N4
• Calculated formula: C48 H88 Ce N4
• Title of publication: Facile formation of a homoleptic Ce(iv) amide via aerobic oxidation
• Authors of publication: Hitchcock, Peter B.; Lappert, Michael F.; Protchenko, Andrey V.
• Journal of publication: Chemical Communications
• Year of publication: 2006
• Journal issue: 33
• Pages of publication: 3546 - 3548
• a: 21.1876 ± 0.0005 Å
• b: 21.1876 ± 0.0005 Å
• c: 10.3198 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4632.7 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 81
• Hermann-Mauguin space group symbol: P -4
• Hall space group symbol: P -4
• Residual factor for all reflections: 0.0746
• Residual factor for significantly intense reflections: 0.0484
• Weighted residual factors for significantly intense reflections: 0.0956
• Weighted residual factors for all reflections included in the refinement: 0.106
• Goodness-of-fit parameter for all reflections included in the refinement: 1.006
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No