Information card for entry 7111561

Structure parameters

• Formula: C38 H54 Ge2 N4 Si4
• Calculated formula: C38 H54 Ge2 N4 Si4
• SMILES: [Ge]1([Ge]2[n]3ccccc3C([Si](C)(C)C)=C(N2[Si](C)(C)C)c2ccccc2)[n]2ccccc2C([Si](C)(C)C)=C(N1[Si](C)(C)C)c1ccccc1
• Title of publication: Synthesis of a germanium analogue of a dithiocarboxylic acid anhydride from the Ge(i) pyridyl-1-azaallyl dimer
• Authors of publication: Leung, Wing-Por; Chiu, Wang-Kin; Chong, Kim-Hung; Mak, Thomas C. W.
• Journal of publication: Chemical Communications
• Year of publication: 2009
• Journal issue: 44
• Pages of publication: 6822 - 6824
• a: 13.346 ± 0.003 Å
• b: 11.006 ± 0.003 Å
• c: 15.589 ± 0.004 Å
• α: 90°
• β: 108.301 ± 0.004°
• γ: 90°
• Cell volume: 2174 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0516
• Residual factor for significantly intense reflections: 0.0397
• Weighted residual factors for significantly intense reflections: 0.0913
• Weighted residual factors for all reflections included in the refinement: 0.0984
• Goodness-of-fit parameter for all reflections included in the refinement: 0.967
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No