Information card for entry 7111748

Structure parameters

• Formula: C40 H36 Fe4 P4
• Calculated formula: C40 H36 Fe4 P4
• Title of publication: Stoichiometric and catalytic Sn-mediated dehydrocoupling of primary phosphines
• Authors of publication: Naseri, Vesal; Less, Robert J.; Mulvey, Robert E.; McPartlin, Mary; Wright, Dominic S.
• Journal of publication: Chemical Communications
• Year of publication: 2010
• Journal volume: 46
• Journal issue: 27
• Pages of publication: 5000 - 5002
• a: 11.652 ± 0.0016 Å
• b: 11.652 ± 0.0016 Å
• c: 6.2473 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 848.2 ± 0.2 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 4
• Space group number: 81
• Hermann-Mauguin space group symbol: P -4
• Hall space group symbol: P -4
• Residual factor for all reflections: 0.0421
• Residual factor for significantly intense reflections: 0.0412
• Weighted residual factors for significantly intense reflections: 0.1065
• Weighted residual factors for all reflections included in the refinement: 0.1077
• Goodness-of-fit parameter for all reflections included in the refinement: 1.092
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No