Information card for entry 7111750

Structure parameters

• Formula: C52 H48 Cl4 Fe4 P4 Sn4
• Calculated formula: C52 H49 Cl4 Fe4 P4 Sn4.12
• Title of publication: Stoichiometric and catalytic Sn-mediated dehydrocoupling of primary phosphines
• Authors of publication: Naseri, Vesal; Less, Robert J.; Mulvey, Robert E.; McPartlin, Mary; Wright, Dominic S.
• Journal of publication: Chemical Communications
• Year of publication: 2010
• Journal volume: 46
• Journal issue: 27
• Pages of publication: 5000 - 5002
• a: 18.245 ± 0.004 Å
• b: 15.165 ± 0.003 Å
• c: 19.997 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5533 ± 2 ų
• Cell temperature: 260 ± 2 K
• Ambient diffraction temperature: 260 ± 2 K
• Number of distinct elements: 6
• Space group number: 63
• Hermann-Mauguin space group symbol: C m c m
• Hall space group symbol: -C 2c 2
• Residual factor for all reflections: 0.0568
• Residual factor for significantly intense reflections: 0.0363
• Weighted residual factors for significantly intense reflections: 0.0891
• Weighted residual factors for all reflections included in the refinement: 0.1002
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No