Information card for entry 7111952

Structure parameters

• Formula: C24 H27 O8 P
• Calculated formula: C24 H27 O8 P
• SMILES: P(=O)([C@H]1CO[C@@H]([C@H]([C@@H]1OC(=O)C)OC(=O)C)COC(=O)C)(c1ccccc1)c1ccccc1
• Title of publication: Novel regio- and stereoselective phosphonyl radical addition to glycals promoted by Mn(II)-air: syntheses of 1,2-dideoxy 2-C-diphenylphosphinylglycopyranosides
• Authors of publication: Fuyi Zhang; Liming Wang; Cui Zhang; Yufen Zhao
• Journal of publication: Chem.Commun.
• Year of publication: 2014
• Journal volume: 50
• Pages of publication: 2046
• a: 11.64595 ± 0.00008 Å
• b: 11.64595 ± 0.00008 Å
• c: 31.3727 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 3684.96 ± 0.05 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 169
• Hermann-Mauguin space group symbol: P 61
• Hall space group symbol: P 61
• Residual factor for all reflections: 0.0384
• Residual factor for significantly intense reflections: 0.0365
• Weighted residual factors for significantly intense reflections: 0.0978
• Weighted residual factors for all reflections included in the refinement: 0.0995
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No