Information card for entry 7111956

Structure parameters

• Formula: C54 H67 Ge P
• Calculated formula: C54 H66.763 Ge P
• Title of publication: Activation of gaseous PH3 with low coordinate diaryltetrylene compounds
• Authors of publication: Jonathan W. Dube; Zachary D. Brown; Christine A. Caputo; Philip P. Power; Paul J. Ragogna
• Journal of publication: Chem.Commun.
• Year of publication: 2014
• Journal volume: 50
• Pages of publication: 1944
• a: 14.813 ± 0.003 Å
• b: 19.868 ± 0.004 Å
• c: 16.899 ± 0.003 Å
• α: 90°
• β: 111.25 ± 0.03°
• γ: 90°
• Cell volume: 4635.3 ± 1.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0751
• Residual factor for significantly intense reflections: 0.0583
• Weighted residual factors for significantly intense reflections: 0.1449
• Weighted residual factors for all reflections included in the refinement: 0.1563
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No