Information card for entry 7112020

Structure parameters

• Formula: C47.5 H56 Br N Si Sn
• Calculated formula: C47.5 H56 Br N Si Sn
• Title of publication: A singly bonded amido-distannyne: H2 activation and isocyanide coordination
• Authors of publication: Terrance J. Hadlington; Cameron Jones
• Journal of publication: Chem.Commun.
• Year of publication: 2014
• Journal volume: 50
• Pages of publication: 2321
• a: 9.9346 ± 0.0004 Å
• b: 13.1778 ± 0.0005 Å
• c: 17.8089 ± 0.0008 Å
• α: 72.26 ± 0.002°
• β: 74.655 ± 0.002°
• γ: 71.45 ± 0.002°
• Cell volume: 2068.62 ± 0.15 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0439
• Residual factor for significantly intense reflections: 0.0409
• Weighted residual factors for significantly intense reflections: 0.1071
• Weighted residual factors for all reflections included in the refinement: 0.1082
• Goodness-of-fit parameter for all reflections included in the refinement: 1.183
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No