Information card for entry 7112103

Structure parameters

• Formula: C18 H22 Ge N2
• Calculated formula: C18 H22 Ge N2
• Title of publication: Unusual formation of a N-heterocyclic germylene via homolytic cleavage of a C-C bond
• Authors of publication: Yan Li; Kartik Chandra Mondal; Peter Stollberg; Hongping Zhu; Herbert W. Roesky; Regine Herbst-Irmer; Dietmar Stalke; Heike Fliegl
• Journal of publication: Chem.Commun.
• Year of publication: 2014
• Journal volume: 50
• Pages of publication: 3356
• a: 24.693 ± 0.003 Å
• b: 10.903 ± 0.002 Å
• c: 27.84 ± 0.003 Å
• α: 90°
• β: 114.96 ± 0.02°
• γ: 90°
• Cell volume: 6795 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0442
• Residual factor for significantly intense reflections: 0.0343
• Weighted residual factors for significantly intense reflections: 0.0772
• Weighted residual factors for all reflections included in the refinement: 0.0809
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.56086 Å
• Diffraction radiation type: AgKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No