Information card for entry 7112252

Structure parameters

• Formula: C24 H47 P Si4
• Calculated formula: C24 H47 P Si4
• SMILES: [Si]12([Si](P([Si]1(C(C)C)C(C)C)[Si]2(C(C)C)C(C)C)(C(C)C)C(C)C)c1ccccc1
• Title of publication: Branched tetrasilane substituted phosphines ‒ synthesis and characterisation of PhSi(SiiPr2)3P and {PhSi(SiMe2)3}2P14
• Authors of publication: Michael Feierabend; Carsten von Hanisch
• Journal of publication: Chem.Commun.
• Year of publication: 2014
• Journal volume: 50
• Pages of publication: 4416
• a: 9.164 ± 0.003 Å
• b: 10.207 ± 0.003 Å
• c: 16.441 ± 0.009 Å
• α: 92.88 ± 0.04°
• β: 94.84 ± 0.04°
• γ: 110.34 ± 0.02°
• Cell volume: 1431.6 ± 1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0289
• Residual factor for significantly intense reflections: 0.0247
• Weighted residual factors for significantly intense reflections: 0.0657
• Weighted residual factors for all reflections included in the refinement: 0.0673
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No