Information card for entry 7112317

Structure parameters

• Formula: C68 H106 Fe2 P10 Sm2
• Calculated formula: C68 H106 Fe2 P10 Sm2
• Title of publication: P-P bond formation via reductive dimerization of [Cp^*^Fe(η^5^-P~5~)] by divalent samarocenes
• Authors of publication: Li, Tianshu; Gamer, Michael T.; Scheer, Manfred; Konchenko, Sergey N.; Roesky, Peter W.
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2013
• Journal volume: 49
• Journal issue: 22
• Pages of publication: 2183 - 2185
• a: 14.357 ± 0.003 Å
• b: 28.55 ± 0.006 Å
• c: 17.985 ± 0.004 Å
• α: 90°
• β: 95.08 ± 0.03°
• γ: 90°
• Cell volume: 7343 ± 3 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0434
• Residual factor for significantly intense reflections: 0.0337
• Weighted residual factors for significantly intense reflections: 0.0834
• Weighted residual factors for all reflections included in the refinement: 0.0868
• Goodness-of-fit parameter for all reflections included in the refinement: 0.968
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7108924
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No