Information card for entry 7112390

Structure parameters

• Formula: C58 H67 Al2 F Mo2 N4 O8
• Calculated formula: C58 H67 Al2 F Mo2 N4 O8
• Title of publication: Al-H σ-bond coordination: expanded ring carbene adducts of AlH3 as neutral bi- and tri-functional donor ligands.
• Authors of publication: Abdalla, Joseph A. B.; Riddlestone, Ian M.; Tirfoin, Remi; Phillips, Nicholas; Bates, Joshua I.; Aldridge, Simon
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2013
• Journal volume: 49
• Journal issue: 49
• Pages of publication: 5547 - 5549
• a: 9.8068 ± 0.0001 Å
• b: 17.0565 ± 0.0002 Å
• c: 18.6455 ± 0.0002 Å
• α: 75.1194 ± 0.0004°
• β: 88.9465 ± 0.0004°
• γ: 85.738 ± 0.0004°
• Cell volume: 3005.89 ± 0.06 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0592
• Residual factor for significantly intense reflections: 0.0415
• Weighted residual factors for all reflections: 0.1098
• Weighted residual factors for significantly intense reflections: 0.0917
• Weighted residual factors for all reflections included in the refinement: 0.1098
• Goodness-of-fit parameter for all reflections included in the refinement: 0.9335
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No