Information card for entry 7112432

Structure parameters

• Formula: C52 H40 Ag2 Cl6 N4 O6
• Calculated formula: C52 H40 Ag2 Cl6 N4 O6
• Title of publication: Single-crystal-to-single-crystal direct cross-linking and photopolymerisation of a discrete Ag(I) complex to give a 1D polycyclobutane coordination polymer.
• Authors of publication: Dutta, Saikat; Bučar, Dejan-Krešimir; Elacqua, Elizabeth; MacGillivray, Leonard R.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2013
• Journal volume: 49
• Journal issue: 11
• Pages of publication: 1064 - 1066
• a: 8.7777 ± 0.001 Å
• b: 10.8623 ± 0.0012 Å
• c: 14.2447 ± 0.0015 Å
• α: 101.878 ± 0.005°
• β: 104.271 ± 0.005°
• γ: 98.735 ± 0.005°
• Cell volume: 1258.3 ± 0.2 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.042
• Residual factor for significantly intense reflections: 0.0321
• Weighted residual factors for significantly intense reflections: 0.0849
• Weighted residual factors for all reflections included in the refinement: 0.0892
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7108803
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No