Information card for entry 7112553

Structure parameters

• Formula: C21.5 H23.5 K N3.5 O4 U
• Calculated formula: C21.5 H23.5 K N3.5 O4 U
• Title of publication: New polynuclear U(IV)-U(V) complexes from U(IV) mediated uranyl(V) disproportionation.
• Authors of publication: Mougel, Victor; Pécaut, Jacques; Mazzanti, Marinella
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2012
• Journal volume: 48
• Journal issue: 6
• Pages of publication: 868 - 870
• a: 22.925 ± 0.004 Å
• b: 14.316 ± 0.003 Å
• c: 14.0547 ± 0.0019 Å
• α: 90°
• β: 101.946 ± 0.015°
• γ: 90°
• Cell volume: 4512.8 ± 1.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.172
• Residual factor for significantly intense reflections: 0.0932
• Weighted residual factors for significantly intense reflections: 0.1986
• Weighted residual factors for all reflections included in the refinement: 0.2419
• Goodness-of-fit parameter for all reflections included in the refinement: 0.987
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No