Information card for entry 7112555

Structure parameters

• Formula: C38 H42 N6 O8 U2
• Calculated formula: C38 H42 N6 O8 U2
• Title of publication: New polynuclear U(IV)-U(V) complexes from U(IV) mediated uranyl(V) disproportionation.
• Authors of publication: Mougel, Victor; Pécaut, Jacques; Mazzanti, Marinella
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2012
• Journal volume: 48
• Journal issue: 6
• Pages of publication: 868 - 870
• a: 16.3093 ± 0.0007 Å
• b: 10.8301 ± 0.0002 Å
• c: 22.1561 ± 0.0006 Å
• α: 90°
• β: 105.356 ± 0.003°
• γ: 90°
• Cell volume: 3773.7 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0594
• Residual factor for significantly intense reflections: 0.0377
• Weighted residual factors for significantly intense reflections: 0.0625
• Weighted residual factors for all reflections included in the refinement: 0.0684
• Goodness-of-fit parameter for all reflections included in the refinement: 0.997
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No