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Information card for entry 7112738
Preview
Coordinates | 7112738.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C29 H24 N2 O5 |
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Calculated formula | C29 H24 N2 O5 |
SMILES | c1(ccc(cc1)/C(=C\1C(=O)N(c2ccccc12)C(=O)c1ccccc1)C(=O)C1CCCCC1)N(=O)=O |
Title of publication | Direct beta-acylation of 2-arylidene-1,3-indandiones with acyl chlorides catalyzed by organophosphanes |
Authors of publication | Chia-Jui Lee; Chia-Ning Sheu; Cheng-Che Tsai; Zong-Ze Wu; Wenwei Lin |
Journal of publication | Chem.Commun. |
Year of publication | 2014 |
Journal volume | 50 |
Pages of publication | 5304 |
a | 12.4059 ± 0.0011 Å |
b | 19.6766 ± 0.0016 Å |
c | 10.5992 ± 0.0009 Å |
α | 90° |
β | 109.927 ± 0.003° |
γ | 90° |
Cell volume | 2432.4 ± 0.4 Å3 |
Cell temperature | 200 ± 2 K |
Ambient diffraction temperature | 200 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1083 |
Residual factor for significantly intense reflections | 0.0563 |
Weighted residual factors for significantly intense reflections | 0.1317 |
Weighted residual factors for all reflections included in the refinement | 0.1712 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.025 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7112738.html
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