Information card for entry 7112770

Structure parameters

• Formula: C48 H60 N4 O4 Zn2
• Calculated formula: C48 H60 N4 O4 Zn2
• Title of publication: Reactions of a β-diketiminate zinc hydride complex with heterocumulenes.
• Authors of publication: Schulz, Stephan; Eisenmann, Tamara; Schmidt, Sarah; Bläser, Dieter; Westphal, Ulrich; Boese, Roland
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2010
• Journal volume: 46
• Journal issue: 38
• Pages of publication: 7226 - 7228
• a: 10.4571 ± 0.0003 Å
• b: 13.5684 ± 0.0004 Å
• c: 17.0082 ± 0.0005 Å
• α: 83.802 ± 0.002°
• β: 81.489 ± 0.002°
• γ: 67.819 ± 0.002°
• Cell volume: 2206.45 ± 0.12 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0549
• Residual factor for significantly intense reflections: 0.0497
• Weighted residual factors for significantly intense reflections: 0.122
• Weighted residual factors for all reflections included in the refinement: 0.1247
• Goodness-of-fit parameter for all reflections included in the refinement: 1.106
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No