Information card for entry 7112821

Structure parameters

• Formula: C33 H52 Au B F4 N3
• Calculated formula: C33 H36 Au B F4 N3
• Title of publication: Ligand influence in the selective gold-mediated synthesis of allenes.
• Authors of publication: Nun, Pierrick; Gaillard, Sylvain; Slawin, Alexandra M. Z.; Nolan, Steven P.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2010
• Journal volume: 46
• Journal issue: 48
• Pages of publication: 9113 - 9115
• a: 19.742 ± 0.004 Å
• b: 16.997 ± 0.003 Å
• c: 10.3318 ± 0.0019 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3466.9 ± 1.1 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 6
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0474
• Residual factor for significantly intense reflections: 0.0427
• Weighted residual factors for significantly intense reflections: 0.1092
• Weighted residual factors for all reflections included in the refinement: 0.1111
• Goodness-of-fit parameter for all reflections included in the refinement: 1.258
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No