Information card for entry 7113165

Structure parameters

• Formula: C161 H140 Cl10 Co12 N4 O28 P8 S4
• Calculated formula: C161 H140 Cl10 Co12 N4 O28 P8 S4
• Title of publication: Assembling metals and clusters around an octaphosphine ligand based on N-substituted bis(diphenylphosphanyl)amines: structural characterization of dendrimer-like Co~12~ and Co~16~ branched clusters
• Authors of publication: Rodriguez-Zubiri, Mireia; Gallo, Vito; Rosé, Jacky; Welter, Richard; Braunstein, Pierre
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2008
• Journal issue: 1
• Pages of publication: 64 - 66
• a: 21.034 ± 0.005 Å
• b: 19.519 ± 0.005 Å
• c: 23.247 ± 0.007 Å
• α: 90°
• β: 111.493 ± 0.01°
• γ: 90°
• Cell volume: 8881 ± 4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1655
• Residual factor for significantly intense reflections: 0.0968
• Weighted residual factors for significantly intense reflections: 0.1745
• Weighted residual factors for all reflections included in the refinement: 0.2051
• Goodness-of-fit parameter for all reflections included in the refinement: 1.227
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7102766
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No