Information card for entry 7113231

Structure parameters

• Formula: C105 H87.5 Ag6 Cl9.5 F3 Fe3 O3 P6 S
• Calculated formula: C105 H87.5 Ag6 Cl9.5 F3 Fe3 O3 P6 S
• Title of publication: General formation of trigonal-prismatic [Ag~6~X~5~(dppf)~3~]^+^ (X = Cl, Br, I) through an unusual ligand migration from NiX2(dppf) to AgOTf
• Authors of publication: Teo, Peili; Koh, Lip Lin; Hor, T. S. Andy
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2007
• Journal issue: 41
• Pages of publication: 4221 - 4223
• a: 14.3332 ± 0.0009 Å
• b: 16.8136 ± 0.001 Å
• c: 22.5538 ± 0.0013 Å
• α: 82.969 ± 0.001°
• β: 79.373 ± 0.001°
• γ: 85.157 ± 0.002°
• Cell volume: 5291.2 ± 0.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0681
• Residual factor for significantly intense reflections: 0.0502
• Weighted residual factors for significantly intense reflections: 0.1104
• Weighted residual factors for all reflections included in the refinement: 0.1182
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7102211
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No