Crystallography Open Database

Information card for entry 7113234

Preview

Coordinates	7113234.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40.5 H37 Ag Cl F3 O3 P3 S
Calculated formula	C40.5 H37 Ag Cl F3 O3 P3 S
Title of publication	General formation of trigonal-prismatic [Ag~6~X~5~(dppf)~3~]^+^ (X = Cl, Br, I) through an unusual ligand migration from NiX2(dppf) to AgOTf
Authors of publication	Teo, Peili; Koh, Lip Lin; Hor, T. S. Andy
Journal of publication	Chemical Communications (Cambridge, United Kingdom)
Year of publication	2007
Journal issue	41
Pages of publication	4221 - 4223
a	12.92 ± 0.003 Å
b	24.327 ± 0.006 Å
c	25.854 ± 0.007 Å
α	90°
β	96.581 ± 0.006°
γ	90°
Cell volume	8072 ± 4 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	8
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.2038
Residual factor for significantly intense reflections	0.1548
Weighted residual factors for significantly intense reflections	0.2765
Weighted residual factors for all reflections included in the refinement	0.2993
Goodness-of-fit parameter for all reflections included in the refinement	1.169
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Duplicate of	7102214
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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