Information card for entry 7113335

Structure parameters

• Formula: C72 H80 F24 N8 O24 Pt4 S20
• Calculated formula: C72 H80 F24 N8 O24 Pt4 S20
• Title of publication: Synthesis and structure of a platinum(II) molecular square incorporating four fluxional thiacrown ligands: The crystal structure of [Pt4([9]aneS3)4(4,4'-bipy)4](OTf)8.
• Authors of publication: Janzen, Daron E.; Patel, Ketankumar N.; VanDerveer, Donald G.; Grant, Gregory J.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2006
• Journal issue: 33
• Pages of publication: 3540 - 3542
• a: 33.022 ± 0.007 Å
• b: 13.987 ± 0.003 Å
• c: 26.107 ± 0.005 Å
• α: 90°
• β: 95.24 ± 0.03°
• γ: 90°
• Cell volume: 12008 ± 4 ų
• Cell temperature: 183 ± 2 K
• Ambient diffraction temperature: 183 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0907
• Residual factor for significantly intense reflections: 0.078
• Weighted residual factors for significantly intense reflections: 0.2006
• Weighted residual factors for all reflections included in the refinement: 0.21
• Goodness-of-fit parameter for all reflections included in the refinement: 1.076
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No