Information card for entry 7113368

Structure parameters

• Formula: C29 H61 Li O3 P4
• Calculated formula: C29 H61 Li O3 P4
• Title of publication: [Li(thf)3cyclo-(P4tBu4CH)]‒synthesis, molecular structure and dynamic behaviour.
• Authors of publication: Wolf, Robert; Hey-Hawkins, Evamarie
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2004
• Journal issue: 22
• Pages of publication: 2626 - 2627
• a: 9.996 ± 0.005 Å
• b: 19.104 ± 0.005 Å
• c: 10.29 ± 0.005 Å
• α: 90 ± 0.005°
• β: 113.132 ± 0.005°
• γ: 90 ± 0.005°
• Cell volume: 1807 ± 1.3 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0741
• Residual factor for significantly intense reflections: 0.0628
• Weighted residual factors for significantly intense reflections: 0.1313
• Weighted residual factors for all reflections included in the refinement: 0.1353
• Goodness-of-fit parameter for all reflections included in the refinement: 1.17
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mokα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No