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Information card for entry 7113403
Preview
Coordinates | 7113403.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C27 H30 N2 O4 |
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Calculated formula | C27 H30 N2 O4 |
Title of publication | Enantioselective formal synthesis of uleine alkaloids from phenylglycinol-derived bicyclic lactams. |
Authors of publication | Amat, Mercedes; Pérez, Maria; Llor, Núria; Martinelli, Marisa; Molins, Elies; Bosch, Joan |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2004 |
Journal issue | 14 |
Pages of publication | 1602 - 1603 |
a | 8.931 ± 0.002 Å |
b | 9.599 ± 0.001 Å |
c | 28.08 ± 0.009 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2407.3 ± 1 Å3 |
Cell temperature | 294 ± 2 K |
Ambient diffraction temperature | 294 ± 2 K |
Number of distinct elements | 4 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0981 |
Residual factor for significantly intense reflections | 0.0458 |
Weighted residual factors for significantly intense reflections | 0.1321 |
Weighted residual factors for all reflections included in the refinement | 0.1451 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.968 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7113403.html
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structural data.