Information card for entry 7113440

Structure parameters

• Formula: C48 H74 Lu N3 Si2
• Calculated formula: C48 H65 Lu N3 Si2
• Title of publication: Unusual alkyl group activation and cationic complex formation from a novel lutetium dialkyl complex supported by a tridentate monoanionic ligand
• Authors of publication: Cameron, Thomas M.; Gordon, John C.; Michalczyk, Ryszard; Scott, Brian L.
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2003
• Journal issue: 18
• Pages of publication: 2282 - 2283
• a: 18.45 ± 0.005 Å
• b: 14.22 ± 0.004 Å
• c: 19.167 ± 0.005 Å
• α: 90°
• β: 104.742 ± 0.005°
• γ: 90°
• Cell volume: 4863 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0604
• Residual factor for significantly intense reflections: 0.0533
• Weighted residual factors for significantly intense reflections: 0.0998
• Weighted residual factors for all reflections included in the refinement: 0.1009
• Goodness-of-fit parameter for all reflections included in the refinement: 2.115
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7104800
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No