Information card for entry 7113738

Structure parameters

• Formula: C24.5 H19 B Cl F4 I N2
• Calculated formula: C24.5 H19 B Cl F4 I N2
• Title of publication: Solid state structures of pentacoordinated λ3-iodanes with a trigonal bipyramidal geometry: synthesis of diphenyl- and alkynyl(phenyl)-λ3-iodane complexes with 1,10-phenanthroline
• Authors of publication: Ochiai, Masahito; Suefuji, Takashi; Miyamoto, Kazunori; Shiro, Motoo
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2003
• Journal issue: 12
• Pages of publication: 1438 - 1439
• a: 13.23 ± 0.004 Å
• b: 10.44 ± 0.003 Å
• c: 34.25 ± 0.01 Å
• α: 90°
• β: 97.6 ± 0.03°
• γ: 90°
• Cell volume: 4689 ± 2 ų
• Cell temperature: 93.2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for significantly intense reflections: 0.0704
• Weighted residual factors for all reflections included in the refinement: 0.1959
• Goodness-of-fit parameter for all reflections included in the refinement: 1.372
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoK?a
• Duplicate of: 7103706
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No