Information card for entry 7113756

Structure parameters

• Chemical name: hexa[bis(6,6'-ethynyl-4-pyridine)2,2'-bipyridyl silver penta-cobaltocarborate tetrafluoroborate
• Formula: C178 H220 Ag6 B91 Co5 F4 N28 O1.5
• Calculated formula: C174.656 H204.056 Ag6 B91 Co5 F4.02 N27.352 O0.988
• Title of publication: A novel synthetic strategy for hexanuclear supramolecular architectures
• Authors of publication: Dolomanov, Oleg V.; Blake, Alexander J.; Champness, Neil R.; Schröder, Martin; Wilson, Claire
• Journal of publication: Chemical Communications
• Year of publication: 2003
• Journal issue: 6
• Pages of publication: 682
• a: 15.7177 ± 0.001 Å
• b: 20.1484 ± 0.0012 Å
• c: 20.3876 ± 0.0012 Å
• α: 74.8 ± 0.002°
• β: 70.747 ± 0.0002°
• γ: 86.58 ± 0.0002°
• Cell volume: 5879.6 ± 0.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1251
• Residual factor for significantly intense reflections: 0.0944
• Weighted residual factors for significantly intense reflections: 0.2559
• Weighted residual factors for all reflections included in the refinement: 0.2974
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7104032
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No