Information card for entry 7113770

Structure parameters

• Formula: C83 H137 Li4 N14 Si4
• Calculated formula: C83 H137 Li4 N14 Si4
• Title of publication: An N-lithio-indole from the reaction of LiCH(TMS)2 and PhNC
• Authors of publication: Fernandes, Manuel A.; Lappert, Michael F.; Layh, Marcus; Omondi, Bernard
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2003
• Journal issue: 5
• Pages of publication: 656 - 657
• a: 34.405 ± 0.005 Å
• b: 13.594 ± 0.002 Å
• c: 19.865 ± 0.003 Å
• α: 90°
• β: 92.106 ± 0.002°
• γ: 90°
• Cell volume: 9285 ± 2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0948
• Residual factor for significantly intense reflections: 0.0555
• Weighted residual factors for significantly intense reflections: 0.128
• Weighted residual factors for all reflections included in the refinement: 0.1492
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7104004
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No