Information card for entry 7113796

Structure parameters

• Formula: C36 H51 Cl3 N4 O P2 Pd2 S
• Calculated formula: C36 H50.682 Cl3 N4 O P2 Pd2 S
• Title of publication: Diastereoselective formation of a dipalladium(I) complex supported by a bridging tetradentate ligand, and oxidative addition of RS‒H across a phosphine-bridged Pd^I^‒Pd^I^ bond
• Authors of publication: Foo, S. Jo Ling; Jones, Nathan D.; Patrick, Brian O.; James, Brian R.
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2003
• Journal issue: 8
• Pages of publication: 988 - 989
• a: 9.3678 ± 0.0003 Å
• b: 17.2299 ± 0.0005 Å
• c: 24.7803 ± 0.0009 Å
• α: 90°
• β: 91.755 ± 0.002°
• γ: 90°
• Cell volume: 3997.8 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0455
• Residual factor for significantly intense reflections: 0.03
• Weighted residual factors for significantly intense reflections: 0.0648
• Weighted residual factors for all reflections included in the refinement: 0.0702
• Goodness-of-fit parameter for all reflections included in the refinement: 0.942
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7104072
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No