Information card for entry 7113804

Structure parameters

• Formula: C17 H27 F2 N O Si
• Calculated formula: C17 H27 F2 N O Si
• SMILES: [Si]([C@H]1N(c2ccc(OC)cc2)C[C@@H](C1(F)F)C(C)C)(C)(C)C.[Si]([C@@H]1N(c2ccc(OC)cc2)C[C@H](C1(F)F)C(C)C)(C)(C)C
• Title of publication: Unusual reactions of N-allylic difluoroenamines under thermal conditions
• Authors of publication: Amii, Hideki; Ichihara, Yutaka; Nakagawa, Takashi; Kobayashi, Takeshi; Uneyama, Kenji
• Journal of publication: Chemical Communications
• Year of publication: 2003
• Journal issue: 23
• Pages of publication: 2902
• a: 36.849 ± 0.007 Å
• b: 6.5879 ± 0.0007 Å
• c: 17.015 ± 0.003 Å
• α: 90°
• β: 116.802 ± 0.003°
• γ: 90°
• Cell volume: 3686.8 ± 1 ų
• Cell temperature: 290.2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for significantly intense reflections: 0.0402
• Weighted residual factors for all reflections included in the refinement: 0.0702
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoK=A5a
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No