Information card for entry 7113809

Structure parameters

• Formula: C240 H244 F48 N96 O106 Pb16 S16
• Calculated formula: C240 H160 F48 N96 O106 Pb16 S16
• Title of publication: Self-assembly of a unique hexadecanuclear [4 � (2 � 2)]-Pb16� ?grid of grids? type structureElectronic supplementary information (ESI) available: synthesis of L. See http://www.rsc.org/suppdata/cc/b3/b308512k/
• Authors of publication: Onions, Stuart T.; Frankin, Anthony M.; Horton, Peter N.; Hursthouse, Michael B.; Matthews, Craig J.
• Journal of publication: Chemical Communications
• Year of publication: 2003
• Journal issue: 23
• Pages of publication: 2864
• a: 15.689 ± 0.003 Å
• b: 31.782 ± 0.006 Å
• c: 37.709 ± 0.008 Å
• α: 112.14 ± 0.03°
• β: 93.11 ± 0.03°
• γ: 98.53 ± 0.03°
• Cell volume: 17099 ± 7 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2378
• Residual factor for significantly intense reflections: 0.1256
• Weighted residual factors for significantly intense reflections: 0.2826
• Weighted residual factors for all reflections included in the refinement: 0.3519
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No