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Information card for entry 7113812
Preview
Coordinates | 7113812.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C45 H51 Ge N O3 |
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Calculated formula | C45 H51 Ge N O3 |
SMILES | [Ge]1([C@@H](C(=O)OC)N[C@@H](c2ccccc2)C21c1ccccc1c1ccccc21)(c1c(cc(cc1C)C)C)c1c(cc(cc1C)C)C.CCOCC.[Ge]1([C@H](C(=O)OC)N[C@H](c2ccccc2)C21c1ccccc1c1ccccc21)(c1c(cc(cc1C)C)C)c1c(cc(cc1C)C)C.CCOCC |
Title of publication | The use of a germene for the synthesis of esters of α-germyl-substituted α-amino acid and α-aminophosphonic acid |
Authors of publication | Ech-Cherif El Kettani, S.; Escudié, J.; Couret, C.; Ranaivonjatovo, H.; Lazraq, M.; Soufiaoui, M.; Gornitzka, H.; Cretiu Nemes, G. |
Journal of publication | Chemical Communications (Cambridge, United Kingdom) |
Year of publication | 2003 |
Journal issue | 14 |
Pages of publication | 1662 - 1663 |
a | 11.9777 ± 0.0007 Å |
b | 12.1155 ± 0.0007 Å |
c | 14.554 ± 0.0008 Å |
α | 101.825 ± 0.001° |
β | 95.774 ± 0.001° |
γ | 108.611 ± 0.001° |
Cell volume | 1927.47 ± 0.19 Å3 |
Cell temperature | 193 ± 2 K |
Ambient diffraction temperature | 193 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.038 |
Residual factor for significantly intense reflections | 0.0316 |
Weighted residual factors for significantly intense reflections | 0.083 |
Weighted residual factors for all reflections included in the refinement | 0.0864 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.028 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Duplicate of | 7103758 |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7113812.html
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Users of the data should acknowledge the original authors of the
structural data.