Information card for entry 7113889

Structure parameters

• Formula: C24 H7 B F15 P
• Calculated formula: C24 H7 B F15 P
• SMILES: [PH2](c1ccccc1)[B](c1c(F)c(F)c(F)c(F)c1F)(c1c(F)c(F)c(F)c(F)c1F)c1c(F)c(F)c(F)c(F)c1F
• Title of publication: B(C6F5)3-catalyzed formation of B‒P bonds by dehydrocoupling of phosphine‒boranes
• Authors of publication: Denis, Jean-Marc; Forintos, Henrietta; Szelke, Helga; Toupet, Loic; Pham, Thi-Nhàn; Madec, Pierre-Jean; Gaumont, Annie-Claude
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2003
• Journal issue: 1
• Pages of publication: 54 - 55
• a: 8.07 ± 0.005 Å
• b: 11.337 ± 0.009 Å
• c: 12.992 ± 0.009 Å
• α: 86.66 ± 0.09°
• β: 77.22 ± 0.07°
• γ: 87.56 ± 0.008°
• Cell volume: 1156.7 ± 1.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0989
• Residual factor for significantly intense reflections: 0.0422
• Weighted residual factors for significantly intense reflections: 0.0788
• Weighted residual factors for all reflections included in the refinement: 0.0918
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7103617
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No