Information card for entry 7113925

Structure parameters

• Formula: C82 H24 N O59 S14 Zn17
• Calculated formula: C82 H24 N O59 S14 Zn17
• Title of publication: Cooperative ion-exchange and self-redox process to load catalytic metal nanoparticles into a MOF with Johnson-type cages
• Authors of publication: Tan, Yan-Xi; He, Yan-Ping; Zhang, Jian
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2014
• Journal volume: 50
• Journal issue: 46
• Pages of publication: 6153 - 6156
• a: 24.429 ± 0.005 Å
• b: 24.429 ± 0.005 Å
• c: 45.411 ± 0.011 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 27100 ± 10 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 139
• Hermann-Mauguin space group symbol: I 4/m m m
• Hall space group symbol: -I 4 2
• Residual factor for all reflections: 0.1026
• Residual factor for significantly intense reflections: 0.0939
• Weighted residual factors for significantly intense reflections: 0.2989
• Weighted residual factors for all reflections included in the refinement: 0.3162
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No