Information card for entry 7113939

Structure parameters

• Formula: C36 H40 N4 P2 Se6
• Calculated formula: C36 H40 N4 P2 Se6
• Title of publication: The activation of Woollins' reagent. Isolation of pyridine stabilised PhPSe2
• Authors of publication: Laura Ascherl; Andreas Nordheider; Kasun S. Athukorala Arachchige; David B. Cordes; Konstantin Karaghiosoff; Michael Buhl; Alexandra M. Z. Slawin; J. Derek Woollins
• Journal of publication: Chem.Commun.
• Year of publication: 2014
• Journal volume: 50
• Pages of publication: 6214
• a: 10.406 ± 0.005 Å
• b: 15.548 ± 0.007 Å
• c: 26.232 ± 0.01 Å
• α: 90°
• β: 99.693 ± 0.011°
• γ: 90°
• Cell volume: 4184 ± 3 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for significantly intense reflections: 0.0421
• Weighted residual factors for all reflections included in the refinement: 0.0979
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No