Information card for entry 7113946

Structure parameters

• Formula: C14 H21 Cl5 F10 N4 Si2
• Calculated formula: C14 H21 Cl5 F10 N4 Si2
• Title of publication: Pentacoordinate silicon(IV): cationic, anionic and neutral complexes derived from the reaction of NHC>SiCl4 with highly Lewis acidic (C2F5)2SiH2
• Authors of publication: T. Bottcher; S. Steinhauer; B. Neumann; H-G. Stammler; G.-V. Roschenthaler; B. Hoge
• Journal of publication: Chem.Commun.
• Year of publication: 2014
• Journal volume: 50
• Pages of publication: 6204
• a: 8.1924 ± 0.0002 Å
• b: 12.5273 ± 0.0003 Å
• c: 13.0812 ± 0.0003 Å
• α: 89.833 ± 0.002°
• β: 81.713 ± 0.002°
• γ: 79.902 ± 0.002°
• Cell volume: 1307.56 ± 0.05 ų
• Cell temperature: 99.98 ± 0.1 K
• Ambient diffraction temperature: 99.98 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0247
• Residual factor for significantly intense reflections: 0.024
• Weighted residual factors for significantly intense reflections: 0.062
• Weighted residual factors for all reflections included in the refinement: 0.0625
• Goodness-of-fit parameter for all reflections included in the refinement: 1.101
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No