Information card for entry 7113974

Structure parameters

• Formula: C17 H18 Si
• Calculated formula: C17 H18 Si
• SMILES: C1c2ccccc2C(=C[Si]1(C)C)c1ccccc1
• Title of publication: Silylium ion-promoted dehydrogenative cyclization: synthesis of silicon-containing compounds derived from alkynes
• Authors of publication: Hidekazu Arii; Takashi Kurihara; Kunio Mochida; Takayuki Kawashima
• Journal of publication: Chem.Commun.
• Year of publication: 2014
• Journal volume: 50
• Pages of publication: 6649
• a: 9.8603 ± 0.0013 Å
• b: 10.5873 ± 0.0014 Å
• c: 14.4723 ± 0.0019 Å
• α: 72.748 ± 0.002°
• β: 86.325 ± 0.002°
• γ: 84.298 ± 0.002°
• Cell volume: 1434.8 ± 0.3 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0654
• Residual factor for significantly intense reflections: 0.0449
• Weighted residual factors for significantly intense reflections: 0.0789
• Weighted residual factors for all reflections included in the refinement: 0.0863
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No