Information card for entry 7114006

Structure parameters

• Formula: C44 H57 Co3 Mo8 N12 O48.5 P V8
• Calculated formula: C22 H24 Co1.5 Mo4 N6 O24.25 P0.5 V4
• Title of publication: A novel two-dimensional mixed molybdenum‒vanadium polyoxometalate with two types of cobalt(ii) complex fragments as bridgesElectronic supplementary information (ESI) available: synthesis and characterization of 1. Fig. S1: view of layers down the a axis of 1. Fig. S2: plots of χT and χ‒1 vs. T for 1. See http://www.rsc.org/suppdata/cc/b2/b202540j/
• Authors of publication: Liu, Cai-Ming; Zhang, De-Qing; Xiong, Ming; Zhu, Dao-Ben
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 13
• Pages of publication: 1416
• a: 12.837 ± 0.003 Å
• b: 14.193 ± 0.003 Å
• c: 14.59 ± 0.003 Å
• α: 105.17 ± 0.03°
• β: 114.45 ± 0.03°
• γ: 105.95 ± 0.03°
• Cell volume: 2101.8 ± 1.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0552
• Residual factor for significantly intense reflections: 0.044
• Weighted residual factors for significantly intense reflections: 0.1258
• Weighted residual factors for all reflections included in the refinement: 0.1312
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No