Information card for entry 7114098

Structure parameters

• Formula: C16 H25 N O8
• Calculated formula: C16 H24.375 N O8
• Title of publication: Divergent approach to imino sugar C-glycosides using imino glycals: application to the stereocontrolled synthesis of (+)-deoxoprosophylline
• Authors of publication: Dransfield, Paul J.; Gore, Paul M.; Shipman, Michael; Slawin, Alexandra M. Z.
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 2
• Pages of publication: 150
• a: 8.8915 ± 0.0004 Å
• b: 9.2151 ± 0.0003 Å
• c: 45.8131 ± 0.0019 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3753.7 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0748
• Residual factor for significantly intense reflections: 0.0538
• Weighted residual factors for significantly intense reflections: 0.1252
• Weighted residual factors for all reflections included in the refinement: 0.1345
• Goodness-of-fit parameter for all reflections included in the refinement: 0.987
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No