Information card for entry 7114100

Structure parameters

• Common name: Tb14(OH)18(acac)24
• Formula: C122 H190.6 O66 Tb14
• Calculated formula: C122 H16 O66 Tb14
• Title of publication: Toward constructing nanoscale hydroxo‒lanthanide clusters: syntheses and characterizations of novel tetradecanuclear hydroxo‒lanthanide clusters
• Authors of publication: Wang, Ruiyao; Song, Datong; Wang, Suning
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 4
• Pages of publication: 368
• a: 21.09 ± 0.004 Å
• b: 21.09 ± 0.004 Å
• c: 21.213 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9435 ± 3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 4
• Space group number: 139
• Hermann-Mauguin space group symbol: I 4/m m m
• Hall space group symbol: -I 4 2
• Residual factor for all reflections: 0.0731
• Residual factor for significantly intense reflections: 0.0566
• Weighted residual factors for significantly intense reflections: 0.1409
• Weighted residual factors for all reflections included in the refinement: 0.148
• Goodness-of-fit parameter for all reflections included in the refinement: 1.17
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No