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Information card for entry 7114204
Preview
Coordinates | 7114204.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C53 H74 F9 Gd N8 O16 S3 |
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Calculated formula | C52.25 H66 F8.425 Gd N8 O15.625 S2.925 |
Title of publication | Controlling the variation of axial water exchange rates in macrocyclic lanthanide(iii) complexesElectronic supplementary information (ESI) available: experimental section. See http://www.rsc.org/suppdata/cc/b2/b202862j/ |
Authors of publication | Aime, Silvio; Barge, Alessandro; Batsanov, Andrei S.; Botta, Mauro; Castelli, Daniela Delli; Fedeli, Franco; Mortillaro, Armando; Parker, David; Puschmann, Horst |
Journal of publication | Chemical Communications |
Year of publication | 2002 |
Journal issue | 10 |
Pages of publication | 1120 |
a | 32.018 ± 0.011 Å |
b | 12.654 ± 0.005 Å |
c | 32.715 ± 0.012 Å |
α | 90° |
β | 93.63 ± 0.02° |
γ | 90° |
Cell volume | 13228 ± 8 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 7 |
Space group number | 5 |
Hermann-Mauguin space group symbol | I 1 2 1 |
Hall space group symbol | I 2y |
Residual factor for all reflections | 0.1157 |
Residual factor for significantly intense reflections | 0.0767 |
Weighted residual factors for significantly intense reflections | 0.1908 |
Weighted residual factors for all reflections included in the refinement | 0.2105 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.098 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7114204.html
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