Information card for entry 7114206

Structure parameters

• Formula: C9.6 H9.2 Cu N9 O1.8 W
• Calculated formula: C14 Cu N8 W
• Title of publication: 2-D soft ferromagnet based on [WV(CN)8]3‒ and CuII with a Tc of 34 KElectronic supplementary information (ESI) available: structure of [Cu(tetren)]2+ in 1 and (NC)7W‒CN‒Cu(NC)4 structural motif of 2; table and figures of IR spectra of 1, 2, tetren·5HCl and free tetren. See http://www.rsc.org/suppdata/cc/b2/b202810g/
• Authors of publication: Podgajny, Robert; Korzeniak, Tomasz; Balanda, Maria; Wasiutynski, Tadeusz; Errington, William; Kemp, Terence J.; Alcock, Nathaniel W.; Sieklucka, Barbara
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 10
• Pages of publication: 1138
• a: 7.3792 ± 0.0006 Å
• b: 32.096 ± 0.002 Å
• c: 7.016 ± 0.0006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1661.7 ± 0.2 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 36
• Hermann-Mauguin space group symbol: C m c 21
• Hall space group symbol: C 2c -2
• Residual factor for all reflections: 0.0433
• Residual factor for significantly intense reflections: 0.0419
• Weighted residual factors for significantly intense reflections: 0.0982
• Weighted residual factors for all reflections included in the refinement: 0.099
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No