Information card for entry 7114294

Structure parameters

• Common name: [Bert*Ge(C6H10)(mu-C6H10)]2
• Formula: C90 H128 Ge2
• Calculated formula: C90 H128 Ge2
• Title of publication: Formation of [Ar*Ge{CH2C(Me)C(Me)CH2}CH2C(Me)]2 (Ar* = C6H3-2,6-Trip2; Trip = C6H2-2,4,6-i-Pr3) via reaction of Ar*GeGeAr* with 2,3-dimethyl-1,3-butadiene: evidence for the existence of a germanium analogue of an alkyne
• Authors of publication: Stender, Matthias; Phillips, Andrew D.; Power, Philip P.
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 12
• Pages of publication: 1312
• a: 12.8612 ± 0.0008 Å
• b: 19.4797 ± 0.0012 Å
• c: 16.8275 ± 0.001 Å
• α: 90°
• β: 106.828 ± 0.001°
• γ: 90°
• Cell volume: 4035.3 ± 0.4 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 3
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0991
• Residual factor for significantly intense reflections: 0.0671
• Weighted residual factors for significantly intense reflections: 0.1581
• Weighted residual factors for all reflections included in the refinement: 0.177
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No