Information card for entry 7114327

Structure parameters

• Formula: C18 H32 N Nb Si2
• Calculated formula: C18 H32 N Nb Si2
• Title of publication: Serendipitous syntheses and structures of [Cp2Nb(H){(SiMe2)2(µ-NR)}]
• Authors of publication: Nikonov, Georgii I.; Vyboishchikov, Sergei F.; Kuzmina, Lyudmila G.; Howard, Judith A. K.
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 6
• Pages of publication: 568 - 569
• a: 17.4105 ± 0.0004 Å
• b: 13.2514 ± 0.0003 Å
• c: 8.6175 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1988.17 ± 0.08 ų
• Cell temperature: 150 ± 0.2 K
• Ambient diffraction temperature: 150 ± 0.2 K
• Number of distinct elements: 5
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0545
• Residual factor for significantly intense reflections: 0.05
• Weighted residual factors for all reflections: 0.117
• Weighted residual factors for significantly intense reflections: 0.1122
• Goodness-of-fit parameter for all reflections: 1.228
• Goodness-of-fit parameter for significantly intense reflections: 1.246
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No