Information card for entry 7114398

Structure parameters

• Chemical name: 1,4,7,10,13,16-hexaoxacyclooctadecane- bis(trimethylsilylmethyl)lutetium(III)- trimethylsilylmethyltriphenylborate
• Formula: C43 H74 B Cl Lu O6 Si3
• Calculated formula: C43 H74 B Cl Lu O6 Si3
• Title of publication: The first structurally characterized cationic lanthanide‒alkyl complexesElectronic supplementary information (ESI) available: experimental and spectroscopic details. See http://www.rsc.org/suppdata/cc/b2/b201613n/
• Authors of publication: Arndt, Stefan; Spaniol, Thomas P.; Okuda, Jun
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 8
• Pages of publication: 896
• a: 10.505 ± 0.0005 Å
• b: 16.3955 ± 0.0008 Å
• c: 30.297 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5218.2 ± 0.5 ų
• Cell temperature: 183 ± 2 K
• Ambient diffraction temperature: 183 ± 2 K
• Number of distinct elements: 7
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0666
• Residual factor for significantly intense reflections: 0.0455
• Weighted residual factors for significantly intense reflections: 0.1207
• Weighted residual factors for all reflections included in the refinement: 0.13
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No