Information card for entry 7114406

Structure parameters

• Chemical name: Complex 4(ClO4)3.1.5Et2O.CH3CN
• Formula: C82 H74 Cl3 N7 O13.5 P3 Pt3 S3
• Calculated formula: C82 H56 Cl3 N7 O13.5 P3 Pt3 S3
• Title of publication: Tethered trinuclear cyclometalated platinum(ii) complexes: from crystal engineering to tunable emission energyElectronic supplementary information (ESI) available: schemetic drawings for 1‒4, perspective view of cation of 4(ClO4)3·1.5Et2O·CH3CN and refinement details for X-ray crystallography. See http://www.rsc.org/suppdata/cc/b2/b200723a/
• Authors of publication: Lu, Wei; Zhu, Nianyong; Che, Chi-Ming
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 8
• Pages of publication: 900
• a: 13.134 ± 0.003 Å
• b: 13.463 ± 0.003 Å
• c: 25.34 ± 0.005 Å
• α: 79.99 ± 0.03°
• β: 86.05 ± 0.03°
• γ: 70.32 ± 0.03°
• Cell volume: 4154.5 ± 1.8 ų
• Cell temperature: 301 ± 2 K
• Ambient diffraction temperature: 301 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0862
• Residual factor for significantly intense reflections: 0.058
• Weighted residual factors for significantly intense reflections: 0.1516
• Weighted residual factors for all reflections included in the refinement: 0.1698
• Goodness-of-fit parameter for all reflections included in the refinement: 0.976
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No