Crystallography Open Database

Information card for entry 7114454

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Coordinates	7114454.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C93 H85 Cl3 N12 O8 Pd4
Calculated formula	C88.36 H85 Cl3 N12 O8 Pd4
Title of publication	Architectural formation of a conjugated bimetallic Pd(II) complex via oxidative complexation and a tetracyclic Pd(II) complex via self-assembling complexation
Authors of publication	Moriuchi, Toshiyuki; Kamikawa, Masayuki; Bandoh, Seiji; Hirao, Toshikazu
Journal of publication	Chemical Communications (Cambridge, United Kingdom)
Year of publication	2002
Journal issue	14
Pages of publication	1476 - 1477
a	17.6912 ± 0.0005 Å
b	19.1708 ± 0.0003 Å
c	16.5754 ± 0.0007 Å
α	107.276 ± 0.004°
β	101.263 ± 0.004°
γ	78.927 ± 0.003°
Cell volume	5210.4 ± 0.3 Å³
Cell temperature	296.2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.1403
Weighted residual factors for all reflections included in the refinement	0.3921
Goodness-of-fit parameter for all reflections included in the refinement	1.448
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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