Information card for entry 7114461

Structure parameters

• Formula: C17 H36 Cl3 F3 N3 O3 P S
• Calculated formula: C17 H36 Cl3 F3 N3 O3 P S
• Title of publication: C-Phosphanyl-C-chloroiminium salts as electrophilic carbene synthetic equivalents
• Authors of publication: Merceron, Nathalie; Baceiredo, Antoine; Gornitzka, Heinz; Bertrand, Guy
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 19
• Pages of publication: 2250
• a: 22.8346 ± 0.0014 Å
• b: 58.461 ± 0.003 Å
• c: 8.089 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 10798.3 ± 1.1 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 8
• Space group number: 43
• Hermann-Mauguin space group symbol: F d d 2
• Hall space group symbol: F 2 -2d
• Residual factor for all reflections: 0.0481
• Residual factor for significantly intense reflections: 0.0399
• Weighted residual factors for significantly intense reflections: 0.096
• Weighted residual factors for all reflections included in the refinement: 0.1
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No