Information card for entry 7114525

Structure parameters

• Formula: C216 H226 Eu3 F27 N48 O35 S9
• Calculated formula: C216 H222 Eu3 F27 N48 O35 S9
• Title of publication: The first self-assembled trimetallic lanthanide helicate: different coordination sites in symmetrical molecular architecturesElectronic supplementary information (ESI) available: least-square planes, selected bond distances and bite angles and a figure showing the atomic numbering scheme for [Eu3(C63H65N13O2)3](CF3SO3)9(CH3CN)9(H2O)2. A scheme summarizing the multistep synthesis of L3 and tables collecting ESI-MS and 1H NMR data, and elemental analyses. See http://www.rsc.org/suppdata/cc/b2/b201859d/
• Authors of publication: Bocquet, Bernard; Bernardinelli, Gérald; Ouali, Nadjet; Floquet, Sebastien; Renaud, Fabien; Hopfgartner, Gérard; Piguet, Claude
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 9
• Pages of publication: 930
• a: 14.9286 ± 0.0007 Å
• b: 21.7201 ± 0.0011 Å
• c: 39.2254 ± 0.0017 Å
• α: 96.885 ± 0.005°
• β: 99.428 ± 0.005°
• γ: 104.033 ± 0.006°
• Cell volume: 12002.2 ± 1.1 ų
• Cell temperature: 200 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.055
• Weighted residual factors for all reflections included in the refinement: 0.055
• Goodness-of-fit parameter for all reflections included in the refinement: 1.854
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No