Information card for entry 7114552

Structure parameters

• Common name: {cesium (cyclic hexaethylether Ni(TMTAA) diester)}{cobalt(III) bis(dicarbollide}{dichloromethane}{toluene}
• Formula: C48 H76 B18 Cl2 Co Cs N4 Ni O9
• Calculated formula: C48 H76 B18 Cl2 Co Cs N4 Ni O9
• Title of publication: Ni(ii) N4-macrocycle grafted crown ether: caesium cobalt(iii) bis(dicarbollide) coordination polymer
• Authors of publication: Malic, Nino; Nichols, Peter J.; Raston, Colin L.
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 1
• Pages of publication: 16
• a: 12.067 ± 0.002 Å
• b: 17.667 ± 0.004 Å
• c: 29.266 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6239 ± 2 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 9
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.12
• Residual factor for significantly intense reflections: 0.0629
• Weighted residual factors for significantly intense reflections: 0.1308
• Weighted residual factors for all reflections included in the refinement: 0.149
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No